Sodium Hydroxide → 1-Hydroxymethyl-7-Methoxynaphthalene

HRID 976452Notes

Reaction equation

HRID 976452 reaction equation
C([O:4][CH2:5][C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[C:13]([O:16][CH3:17])[CH:14]=2)[CH:9]=[CH:8][CH:7]=1)(=O)C.[OH-].[Na+]>CO.O>[OH:4][CH2:5][C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[C:13]([O:16][CH3:17])[CH:14]=2)[CH:9]=[CH:8][CH:7]=1

Participants

5

Reactant 2

HCID 14798Sodium HydroxideHCID 185132061-Acetoxymethyl-7-methoxynaphthalene

Product 1

HCID 154530791-Hydroxymethyl-7-Methoxynaphthalene

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

0.1 mole of the preceding 1-acetoxymethyl-7-methoxynaphthalene is saponified at room temperature, under argon, with a solution of 0.2 mole of sodium hydroxide diluted in 200 cm3 of methanol and 40 cm3 of water.

Sources & evidence

ORD record
ord-c7858ff66c474cedae2a0fa4842da4c7
Source dataset
uspto-grants-1997_03
Patent number
US05612368

Reaction notes

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