Acetyl chloride → HCID 19967338, compound

HRID 976454Notes

Reaction equation

HRID 976454 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[CH2:13][O:14][NH:15][C:16](=[O:18])[CH3:17].[C:19](Cl)(=O)[CH3:20].C(Cl)(=O)CCC>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[CH2:13][O:14][NH:15][C:16](=[O:18])[CH2:17][CH2:19][CH3:20]

Participants

4

Reactant 3

HCID 6367Acetyl chlorideHCID 8855Butyryl chlorideHCID 19967247HCID 19967247, compound

Product 1

HCID 19967338HCID 19967338, compound

Procedure

By carrying out the procedure in the same manner as for the synthesis of the compound of Example 7, but replacing, in the acylation step, acetic acid chloride with butyric acid chloride, the title compound is obtained.

Sources & evidence

ORD record
ord-0eaba846376b421bb6c7b301aaa94455
Source dataset
uspto-grants-1997_03
Patent number
US05612368

Reaction notes

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