Acetyl chloride → HCID 19967269, compound

HRID 976455Notes

Reaction equation

HRID 976455 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[CH2:13][O:14][NH:15][C:16](=[O:18])[CH3:17].[C:19](Cl)(=O)[CH3:20].C(Cl)(=O)/C=C/C>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]=1[CH2:13][O:14][NH:15][C:16](=[O:18])/[CH:17]=[CH:19]/[CH3:20]

Participants

4

Reactant 3

HCID 6367Acetyl chlorideHCID 643131trans-Crotonyl chlorideHCID 19967247HCID 19967247, compound

Product 1

HCID 19967269HCID 19967269, compound

Procedure

By carrying out the procedure in the same manner as for the synthesis of the compound of Example 7, but replacing, in the acylation step, acetic acid chloride with crotonic acid chloride, the title compound is obtained.

Sources & evidence

ORD record
ord-2b83eb60e5e74a049597a1fc102a45f3
Source dataset
uspto-grants-1997_03
Patent number
US05612368

Reaction notes

Loading…