HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 19967263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Nitrobenzene | HCID 7416 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 9837740 | HCID 9837740 | — |
| Product | HCID 19967263 | HCID 19967263 | — |
Reaction Steps
Starting with a solution of the compound of Example 1 and AlCl3, in a solvent such as nitrobenzene, acetyl chloride is added dropwise at 12° C. and under nitrogen. The reaction is allowed to proceed for 2 hours at 12° C. and the reaction mixture is poured over ice. The crude mixture is extracted, dried, concentrated and chromatographed on silica. The title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612368 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-15a64a22caf14c80b486e83bd94d7697 |
| Source note | uspto-grants-1997_03 |