HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → (Benzyloxy)(methyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | tert-butyl N-benzyloxy-N-methylcarbamate | HCID 14227181 | — |
| Reactant | tert-butyl N-benzyloxy-N-(2-methylpropyl)carbamate | HCID 19967428 | — |
| Product | (Benzyloxy)(methyl)amine | HCID 13417387 | — |
Reaction Steps
Using the general method of Compound 54 Part C, tert-butyl N-benzyloxy-N-methylcarbamate (3.0 g, 13 mmol) was reacted with trifluoroacetic acid (10 mL, 130 mmol) to provide 1.58 g of N-benzyloxy-N-methylamine as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612377 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-dfca262cc7444a829f0c340430c1b57e |
| Source note | uspto-grants-1997_03 |