4-Bromoheptane → 1-Benzyloxy-1-(1-propylbutyl)-3-phenylurea

HRID 976639Notes

Reaction equation

HRID 976639 reaction equation
Br[CH:2]([CH2:6][CH2:7][CH3:8])[CH2:3][CH2:4][CH3:5].[CH2:9]([O:16][NH:17][C:18]([NH:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)=[O:19])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH2:9]([O:16][N:17]([CH:2]([CH2:6][CH2:7][CH3:8])[CH2:3][CH2:4][CH3:5])[C:18]([NH:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)=[O:19])[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 704604-BromoheptaneHCID 2542991-(Benzyloxy)-3-phenylurea

Product 1

HCID 199674341-Benzyloxy-1-(1-propylbutyl)-3-phenylureaYield 38.9%

Procedure

Using the general method of Compound 42 Part B, 4-bromoheptane (5.84 g, 32.6 mmole) was reacted with 1-benzyloxy-3-phenylurea (7.3 g, 30.2 mmole) to provide about 4 g of 1-benzyloxy-1-(1-propylbutyl)-3-phenylurea.

Sources & evidence

ORD record
ord-2f3d90ffc6d04d03899236561a28cadf
Source dataset
uspto-grants-1997_03
Patent number
US05612377

Reaction notes

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