3-Bromopentane → HCID 19967414, compound

HRID 976643Notes

Reaction equation

HRID 976643 reaction equation
[C:1]([O:5][C:6](=[O:20])[N:7]([O:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[CH2:8][CH:9]([CH3:11])C)([CH3:4])([CH3:3])[CH3:2].Br[CH:22](CC)[CH2:23]C.C(ONC(=O)OC(C)(C)C)C1C=CC=CC=1>>[CH2:13]([O:12][N:7]([CH:8]([CH2:9][CH3:11])[CH2:22][CH3:23])[C:6](=[O:20])[O:5][C:1]([CH3:2])([CH3:3])[CH3:4])[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1

Participants

4

Reactant 3

HCID 157383-BromopentaneHCID 736159Tert-butyl N-(benzyloxy)carbamateHCID 19967428tert-butyl N-benzyloxy-N-(2-methylpropyl)carbamate

Product 1

HCID 19967414HCID 19967414, compound

Procedure

Using the general method of Compound 54 Part B, 3-bromopentane (15.0 mL, 121 mmole) was reacted with tert-butyl N-benzyloxycarbamate (25.1 g, 112 mmole) to provide tert-butyl N-benzyloxy-N-(1-ethylpropyl)carbamate.

Sources & evidence

ORD record
ord-e80de2af317a48d68b251509f2db3916
Source dataset
uspto-grants-1997_03
Patent number
US05612377

Reaction notes

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