HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 10130617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 2,4-Diamino-6-chloropyrimidine | HCID 67432 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 10130617 | HCID 10130617 | — |
Reaction Steps
A solution of 3.8 g sodium in 100 mL benzylalcohol is heated in an oil bath with 21.6 g 6-chloro-2,4-diamino-pyrimidine (6) for 3 hours at 160° C. The surplus alcohol is distilled off in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05612468 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-8425590bb7994c54a64dd0d775814fa6 |
| Source note | uspto-grants-1997_03 |