HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 976941Generated: October 29, 2026
Benzoyl chloride → HCID 19967563, compound
https://huagongshe.com/reaction/976941
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 4-Amino-7-methylpteridin-2(3H)-one | HCID 178430061 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19967563 | HCID 19967563 | — |
Reaction Steps
In 20 mL of pyridine is dissolved 1.63 g (0.01 mole) of 4-amino-7-methyl-pteridine-2-one (20). Then 3.12 g (0.02 mole) of benzoyl chloride is added dropwise while stirring the mixture. The mixture is heated to 80° C. for 30 minutes and then poured on ice. The resulting precipitate is collected, washed with ethanol and ether and then recrystallized from DMF to give 21.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05612468 |
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| Source dataset | uspto-grants-1997_03 |
|---|
| ORD ID | ord-e994a31b910143b6ade8eccccc03bf34 |
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| Source note | uspto-grants-1997_03 |
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