Myristic Acid → Myristoyl chloride

HRID 977071Notes

Reaction equation

HRID 977071 reaction equation
[C:1]([OH:16])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].S(Cl)([Cl:19])=O>ClC=C(Cl)Cl>[C:1]([Cl:19])(=[O:16])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

4

Reactant 2

HCID 11005Myristic AcidHCID 24386Thionyl Chloride

Product 1

HCID 66986Myristoyl chloride

Reagents, catalysts & solvents 1

HCID 6575TrichloroethyleneSolvent

Procedure

Myristoyl chloride was synthesized by refluxing myristic acid (7.0 g) and thionyl chloride (9 ml) in trichloroethylene (100 ml) for 3 h. The solvent was then evaporated.

Workup

  1. customThe solvent was then evaporated

Sources & evidence

ORD record
ord-a539d15b34814817a38b73d051575aab
Source dataset
uspto-grants-1997_03
Patent number
US05614514

Reaction notes

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