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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 977256Generated: October 31, 2026

Diisobutylaluminumhydride → HCID 19965667, compound

https://huagongshe.com/reaction/977256

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisobutylaluminumhydrideHCID 21225700—
ReactantHCID 86750604HCID 86750604—
ProductHCID 19965667HCID 19965667—

Reaction Steps

Ethyl (E)-4-[2-(5-methyl-2-phenyl-4-oxazolyl)vinyl]cinnamate was reduced with diisobutylaluminum hydride in the same manner as in Reference Example 22 to yield (E,E)-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)vinyl]phenyl]-2-propenol, which was then recrystallized from ethyl acetate to yield light yellow prisms having a melting point of 165°-166° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05614544
Source datasetuspto-grants-1997_03
ORD IDord-96f86f620b4648a7b5947bb21bcb5ac0
Source noteuspto-grants-1997_03