HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 19965628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 53981278 | HCID 53981278 | — |
| Product | HCID 19965628 | HCID 19965628 | — |
Reaction Steps
Ethyl 4-[2-(5-methyl-4-phenyl-2-thiazolyl)ethyl]cinnamate was reduced with diisobutylaluminum hydride in the same manner as in Reference Example 22 to yield (E)-3-[4-[2-(5-methyl-4-phenyl-2thiazolyl)ethyl]phenyl]-2-propenol, which was then recrystallized from hexane to yield colorless plates having a melting point of 93°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614544 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-9c450fc7d8374b8dad1e8c070207627c |
| Source note | uspto-grants-1997_03 |