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Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate → 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate | HCID 19965620 | — |
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 生成物 | 4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol | HCID 54568002 | — |
反応手順
Methyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzoate was reduced with lithium aluminum hydride in the same manner as in Reference Example 12 to yield 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]benzyl alcohol, which was then recrystallized from ethyl acetate-hexane to yield colorless plates having a melting point of 103°-104° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05614544 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-75b253952b1443f8887904166dc53a19 |
| 出典メモ | uspto-grants-1997_03 |