HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 19965629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 54015069 | HCID 54015069 | — |
| Product | HCID 19965629 | HCID 19965629 | — |
Reaction Steps
Ethyl 4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]cinnamate was reduced with diisobutylaluminum hydride in the same manner as in Reference Example 22 to yield (E)-3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]phenyl]2-propenol, which was then recrystallized from ethyl acetate-hexane to yield colorless needles having a melting point of 102°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614544 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-6a7becfc0095414b83d2feae46dd370b |
| Source note | uspto-grants-1997_03 |