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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 977268Generated: October 31, 2026

Diisobutylaluminumhydride → HCID 19965658, compound

https://huagongshe.com/reaction/977268

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisobutylaluminumhydrideHCID 21225700—
ReactantHCID 86750608HCID 86750608—
ProductHCID 19965658HCID 19965658—

Reaction Steps

Ethyl (E,E)-5-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethyl]phenyl]-2,4pentadienoate was reduced with diisobutylaluminum hydride in the same manner as in Reference Example 22 to yield (E,E)-5-[4-[2-(5-methyl-2-phenyl4-oxazolyl)ethyl]phenyl]-2,4-pentadien-1-ol, which was then recrystallized from ethyl acetate-hexane to yield colorless prisms having a melting point of 117°-118° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05614544
Source datasetuspto-grants-1997_03
ORD IDord-fe7157686b4e42a09fc8e1c71b416e10
Source noteuspto-grants-1997_03