HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 19965621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 86750611 | HCID 86750611 | — |
| Product | HCID 19965621 | HCID 19965621 | — |
Reaction Steps
Ethyl (E,E,E)-5-[4-[2-[2-(2-furyl)-5-methyl-4-oxazolyl]vinyl]phenyl]2,4-pentadienoate was reduced with diisobutylaluminum hydride in the same manner as in Reference Example 22 to yield (E,E,E)-5-[4-[2-[2-(2-furyl)-5-methyl-4-oxazolyl]vinyl]phenyl]-2,4-pentadien-1-ol, which was then recrystallized from ethyl acetate to yield colorless needles having a melting point of198°-199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614544 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-d2e1d285ed744d9fb7d964ccaecd55c0 |
| Source note | uspto-grants-1997_03 |