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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 977398Generated: October 31, 2026

Potassium Carbonate → HCID 21268313, compound

https://huagongshe.com/reaction/977398

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-(3-chloropropoxy)-1H-indoleHCID 11694169—
Reactant6-Nitro-3-(1,2,3,6-tetrahydro-4-pyridinyl)-1H-indoleHCID 21268269—
ProductHCID 21268313HCID 21268313—

Reaction Steps

The title compound was prepared in a fashion similar to that described in Example 192 from 6-nitro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole (0.50 g, 2.1 mmol), 1-chloro-3-(1H-indole-4-oxy)propane (0.43 g, 2.1 mmol) and potassium carbonate (0.32 g, 2.3 mmol). The product was isolated as an orange granular solid. Yield 0.49 g (56%). mp 215°-225° C. FDMS m/e=416 (M+ of free base).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05614523
Source datasetuspto-grants-1997_03
ORD IDord-b0f8ea73caa548a0bf7571802f279c52
Source noteuspto-grants-1997_03