HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21268320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-methyl-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 10420726 | — |
| Reactant | 4-(3-chloropropoxy)-1H-indole | HCID 11694169 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21268320 | HCID 21268320 | — |
Reaction Steps
The title compound was prepared in a fashion similar to that described in Example 99 using 1-chloro-3-(1H-indole-4-oxy)propane (0.273 g, 2.4 mmol) and 6-methyl-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole (0.279 g, 2.4 mmol) in the presence of 2.0 equivalents of K2CO3 (0.593, 4.3 mmol) in dimethylformamide at 90° C. Yield 0.167 g (50%) of a tan powder. mp C. FDMS m/e=405 (M+ of free base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614523 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-eb32872cd84b44d9b0cbfe350dbfb49e |
| Source note | uspto-grants-1997_03 |