HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2-[3,5-bis-(Carboxy)-benzoyl]-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-[3,5-bis-(Methoxycarbonyl)-benzoyl]-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine | HCID 15661745 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-[3,5-bis-(Carboxy)-benzoyl]-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine | HCID 15661747 | 31.9% |
Reaction Steps
Under the conditions of example 2, 20 mg of 2-[3,5-bis-(methoxycarbonyl)-benzoyl]-6-[(1E)-(3RS)-3-hydroxy-1-undecenyl]-pyridine in 2 ml of methanol is saponified with 2 ml of 1 n sodium hydroxide solution and worked up. 6 mg of the title compound is obtained as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614634 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-ed6d1b8e6e4841678f375b5adc513d62 |
| Source note | uspto-grants-1997_03 |