HRID977890

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID4265726

2,2-dimethyldodecanoic Acid

C14H28O2

结构：CC(C)(C)c1ccc(CCC(CC2CCCCC2)O[Si](C)(C)C(C)(C)C)cc1N

HCID19966217

未命名化合物

PRODUCTS

生成物

结构：CCCCCCCCCCC(C)(C)C(=O)Nc1cc(CCC(CC2CCCCC2)O[Si](C)(C)C(C)(C)C)ccc1C(C)(C)C

HCID19966100

未命名化合物

PROCEDURE

实验过程

Following a procedure similar to that described in Example 21, but using 2,2-dimethyldodecanoic acid and 2-t-butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]aniline [prepared by a procedure similar to that described in Preparation 11(i)] as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a foam-like material.

WORKUP

后处理

customprepared by a procedure similar to

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-5664072b131b4b979723bb87811ca586
来源数据集: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05614550
来源说明: uspto-grants-1997_03

反应 SMILES

[CH3:1][C:2]([CH3:16])([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=O.[C:17]([C:21]1[CH:27]=[CH:26][C:25]([CH2:28][CH2:29][CH:30]([O:38][Si:39]([C:42]([CH3:45])([CH3:44])[CH3:43])([CH3:41])[CH3:40])[CH2:31][CH:32]2[CH2:37][CH2:36][CH2:35][CH2:34][CH2:33]2)=[CH:24][C:22]=1[NH2:23])([CH3:20])([CH3:19])[CH3:18]>>[C:17]([C:21]1[CH:27]=[CH:26][C:25]([CH2:28][CH2:29][CH:30]([O:38][Si:39]([C:42]([CH3:45])([CH3:44])[CH3:43])([CH3:41])[CH3:40])[CH2:31][CH:32]2[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37]2)=[CH:24][C:22]=1[NH:23][C:3](=[O:5])[C:2]([CH3:1])([CH3:16])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])([CH3:20])([CH3:18])[CH3:19]