HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86741471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6-Chloropurine riboside | HCID 93003 | — |
| Reactant | HCID 15212223 | HCID 15212223 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86741471 | HCID 86741471 | 98% |
Reaction Steps
A reaction mixture of 1.75 g of 6-chloropurine riboside, 1.78 g of fluorenylethylamine and 1.84 g of triethylamine is refluxed in 50 ml of ethanol under nitrogen for 20 hrs. Upon cooling, solid material crystallizes out. It is filtered and dried affording 2.75 g (95%) of N6 -fluorenylethyl adenosine having a melting point of 120°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663313 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-a953a2498eae4a6da323c74b2b9b05b2 |
| Source note | uspto-grants-1987_05 |