HCID 13579378, compound → HCID 13579382, compound

HRID 978018Notes

Reaction equation

HRID 978018 reaction equation
C[C:2]1[CH:3]=[CH:4][C:5]([CH:9]2[CH2:11][CH2:10]2)=[C:6]([OH:8])[CH:7]=1.[Cl:12]C1C=CC(C2CC2)=C(C=1)N>[Hg]>[Cl:12][C:2]1[CH:3]=[CH:4][C:5]([CH:9]2[CH2:11][CH2:10]2)=[C:6]([OH:8])[CH:7]=1

Participants

4

Reactant 2

HCID 13579378HCID 13579378, compoundHCID 20204861HCID 20204861, compound

Product 1

HCID 13579382HCID 13579382, compoundYield 32%

Reagents, catalysts & solvents 1

HCID 23931MercuryCatalyst

Procedure

Prepared according to the method described for the 5-methyl-2-cyclopropyl-phenol of Example I, from 31.5 g (0.188 mol/g) of 5-chloro-2-cyclopropyl-aniline with a yield of 32%. B.P.=69° C.-76° C./0.1 mm mercury. m.P. 30° C.

Workup

  1. customPrepared
  2. customm.P. 30° C.

Sources & evidence

ORD record
ord-5b652c9e9bd046b48c7050aad4dc9ae2
Source dataset
uspto-grants-1987_05
Patent number
US04663340

Reaction notes

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