HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycine → HCID 10176752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycine | HCID 750 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Nonanoyl chloride | HCID 69819 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10176752 | HCID 10176752 | 79.5% |
Reaction Steps
Glycine (20 mmol) was reacted with nonanoyl chloride (22 ml) in the presence of NaOH (40 mmol) in a mixture of water and ether as described in Example 1 Part A. The crude crystalline product (4.25 g) was recrytallized from ethyl acetate (40-50 ml) to give the title compound (3.42 g, 79.5%), m.p. 106°-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663336 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-e9d984d4bac247a1b4a1b4d511b3463f |
| Source note | uspto-grants-1987_05 |