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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 978055Generated: October 29, 2026

Glycine → HCID 10176752, compound

https://huagongshe.com/reaction/978055

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlycineHCID 750—
ReactantEthyl AcetateHCID 8857—
ReactantSodium HydroxideHCID 14798—
ReactantNonanoyl chlorideHCID 69819—
SolventWaterHCID 962—
SolventDiethyl EtherHCID 3283—
ProductHCID 10176752HCID 1017675279.5%

Reaction Steps

Glycine (20 mmol) was reacted with nonanoyl chloride (22 ml) in the presence of NaOH (40 mmol) in a mixture of water and ether as described in Example 1 Part A. The crude crystalline product (4.25 g) was recrytallized from ethyl acetate (40-50 ml) to give the title compound (3.42 g, 79.5%), m.p. 106°-109° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04663336
Source datasetuspto-grants-1987_05
ORD IDord-e9d984d4bac247a1b4a1b4d511b3463f
Source noteuspto-grants-1987_05