HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20142835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Glycine ethyl ester | HCID 12176 | — |
| Reactant | Benzenepentanoic acid | HCID 16757 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20142835 | HCID 20142835 | — |
Reaction Steps
5-Phenylvaleric acid (2.67 g, 15 mmol) in distilled THF was reacted with CDI (15 mmol) followed by glycine ethyl ester.HCl (15 mmol) and (C2H5)3N (15 mmol) as described in Example 56 Part A. The crude material (3.25 g, 82%) was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663336 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-5b4d167472444874aba9d700da25146b |
| Source note | uspto-grants-1987_05 |