HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Acifluorfen sodium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Acifluorfen | HCID 44073 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Acifluorfen sodium | HCID 44072 | 105.4% |
Reaction Steps
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04662935 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-973848e0be8949cca8e2402446870f93 |
| Source note | uspto-grants-1987_05 |