HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Acifluorfen | HCID 44073 | — |
| Product | Dimethylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate | HCID 21280075 | — |
Reaction Steps
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (2.0 g) is dissolved in toluene and an excess of anhydrous dimethylamine is bubbled into the reaction mixture, the solvent removed in vacuo and the residue triturated with cold diethyl ether to give 1.1 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04662935 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-3c5b21367724484295ca9485c34f0d06 |
| Source note | uspto-grants-1987_05 |