HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13883776, compound → HCID 13883778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13883776 | HCID 13883776 | — |
| Reactant | 1,1,1-Trifluoro-2-isothiocyanatoethane | HCID 13883777 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13883778 | HCID 13883778 | — |
Reaction Steps
To a solution of 5-(3-aminopyrazol-1-yl)valeronitrile (7.0 g.) in acetonitrile (25 ml.) was added 2,2,2-trifluoroethylisothiocyanate (6.02 g.). After 15 minutes the solvent was evaporated in vacuo to give 5-(3-[3-(2,2,2-trifluoroethyl)thioureido]pyrazol-1-yl)valeronitrile as a white crystalline solid, m.p. 96°-98°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665073 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-1972cec1303b485db9d1ca3635c12e52 |
| Source note | uspto-grants-1987_05 |