HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178504040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(2,2,2-Trifluoroethyl)thiourea | HCID 20202812 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178504040 | HCID 178504040 | — |
Reaction Steps
A solution of 2,2,2-trifluoroethylthiourea (8.0 g.) and methyl iodide (3.5 g.) in EtOH (40 ml.) was heated under reflux for 70 minutes, then evaporated to dryness in vacuo. The residue was triturated with ether to give 2,2,2-trifluoroethyl-S-methylisothiourea hydroiodide, m.p. 154°-156° (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665073 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-4960a60ca38242b3bae6f6cece2e2d00 |
| Source note | uspto-grants-1987_05 |