Hydrochloric Acid → HCID 131715133, compound

Participants

Reaction Steps

Following the procedure of Example 1-A, 9 grams (0.0448 mole) of cyanuric chloride, 61.29 (0.269 mole) of bisphenol A, and 70.29 grams of methyl ethyl ketone were heated until temperature reached 50° C., then 12.88 grams (0.161 mole) of 50% aqueous caustic was added during about one hour (3600 s). The mixture was digested an additional hour (3600 s) at 60° C. The reaction contents was then cooled to ambient, and neutralized using concentrated hydrochloric acid. The organic phase was then washed with water to remove the salt formed, and the excess solvent removed by vacuum distillation up to 150° C. for 30 minutes (1800 s).

Provenance & Evidence