HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanol → HCID 13117144, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanol | HCID 1031 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 13137234 | HCID 13137234 | — |
| Product | HCID 13117144 | HCID 13117144 | — |
Reaction Steps
Into the same flask as used in Example 1, 2-n-pentyl-3-hydroxy-3-methyl-4-cyclopentenone (0.1 mol; 1 part), n-propanol (5 parts) and p-toluenesulfonic acid (1/20 part) were charged, and the mixture was stirred at a temperature of 40° to 70° C. for 5 hours. After completion of the reaction, the mixture was treated in the same manner as in Example 25 to obtain 2-n-pentyl-3-methyl-4-n-propoxy-2-cyclopentenone. Yield, 96%. nD19 1.4792.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665174 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-0bbb271049044623b64f2cf3f7513a11 |
| Source note | uspto-grants-1987_05 |