HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 13827301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 3-(Dimethylamino)-1-propanol | HCID 76646 | — |
| Reactant | HCID 13827299 | HCID 13827299 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13827301 | HCID 13827301 | — |
Reaction Steps
The acid chloride (25 g) of Example 29 above was dissolved in THF (1250 ml) and 3-dimethylaminopropanol (250 ml) was added dropwise. After stirring overnight at room temperature ether (2 l) was added and the resulting precipitate was filtered. The crude ester (13.6 g) was purified via the hydrochloride salt, mp 288° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665181 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-36196aaaa4f94968a1fbfbf3c2ee2ae1 |
| Source note | uspto-grants-1987_05 |