3-Nitrobenzenesulfonyl chloride → HCID 13913714, compound

HRID 978807Notes

Reaction equation

HRID 978807 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([S:10](Cl)(=[O:12])=[O:11])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[CH:14]([NH:17][CH2:18][CH2:19][CH2:20][NH2:21])([CH3:16])[CH3:15]>>[CH3:15][CH:14]([NH:17][CH2:18][CH2:19][CH2:20][NH:21][S:10]([C:6]1[CH:7]=[CH:8][CH:9]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=1)(=[O:12])=[O:11])[CH3:16]

Participants

3

Reactant 2

HCID 84763-Nitrobenzenesulfonyl chlorideHCID 76888N-Isopropylpropane-1,3-diamine

Product 1

HCID 13913714HCID 13913714, compound

Procedure

Following the procedure of Example 1, m-nitrobenzenesulfonyl chloride was reacted with N-isopropyl propane-1,3-diamine to provide the free base, m.r. 57°-59° C., converted to the hydrochloride salt, m.r. 184°-188° C.

Workup

  1. customto provide the free base, m.r
  2. custom57°-59° C.
  3. custom184°-188° C.

Sources & evidence

ORD record
ord-99bafec258f84041ac698e875194dc8e
Source dataset
uspto-grants-1987_05
Patent number
US04665227

Reaction notes

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