4-Nitrobenzenesulfonyl chloride → N-[2-[bis(1-methylethyl)amino]ethyl]-4-nitrobenzene sulfonamide

HRID 978810Notes

Reaction equation

HRID 978810 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10](Cl)(=[O:12])=[O:11])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH2:20])([CH3:16])[CH3:15]>>[CH3:15][CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH:20][S:10]([C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1)(=[O:12])=[O:11])[CH3:16]

Participants

3

Reactant 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 84591,2-Ethanediamine, N1,N1-bis(1-methylethyl)-

Product 1

HCID 13913719N-[2-[bis(1-methylethyl)amino]ethyl]-4-nitrobenzene sulfonamide

Procedure

Following the procedure of Example 1, p-nitrobenzenesulfonyl chloride was reacted with N,N-diisopropyl ethylene diamine to give the free base, m.r. 86°-88° C.

Workup

  1. customto give the free base, m.r
  2. custom86°-88° C.

Sources & evidence

ORD record
ord-de551280c8c34fdf867d7fe4697e25c8
Source dataset
uspto-grants-1987_05
Patent number
US04665227

Reaction notes

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