HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanesulfinate → HCID 54422945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanesulfinate | HCID 2733271 | — |
| Reactant | HCID 11821934 | HCID 11821934 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54422945 | HCID 54422945 | 41.9% |
Reaction Steps
To a solution of 0.494 g of (3S,4S)-4-acetoxy-3-phenoxyacetamido-2-oxoazetidine in 14 ml of 50% methanol is added 0.51 g of sodium methylsulfinate and the mixture is stirred at room temperature for 18 hours. The methanol is distilled off under reduced pressure to give 222 mg of (3R,4S)-4-methylsulfonyl-3-phenoxyacetamido-2-oxoazetidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665067 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-c4f34dafb5d74c0987e23213f6f19b20 |
| Source note | uspto-grants-1987_05 |