HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86740397, compound → sodium (3R,4S)-4-acetylthio-3-[2-(2-aminothiazol-4-yl)-2-methoxyiminoacetamido]-2-oxoazetidine-1-sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86740397 | HCID 86740397 | — |
| Reactant | HCID 86740408 | HCID 86740408 | — |
| Solvent | Water | HCID 962 | — |
| Product | sodium (3R,4S)-4-acetylthio-3-[2-(2-aminothiazol-4-yl)-2-methoxyiminoacetamido]-2-oxoazetidine-1-sulfonate | HCID 86740407 | 34.1% |
Reaction Steps
To a solution of 0.11 g of sodium (3R,4S)-4-acetylthio-3-[2-(2-chloroacetamidothiazol-4-yl)-2-methoxyiminoacetamido]-2-oxoazetidine-1-sulfonate in 5 ml of water is added under ice-cooling 0.036 g of sodium monomethyldithiocarbamate, and the mixture is stirred at room temperature for 2 hours. The same procedure as Example 3B yields 0.032 g of sodium (3R,4S)-4-acetylthio-3-[2-(2-aminothiazol-4-yl)-2-methoxyiminoacetamido]-2-oxoazetidine-1-sulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665067 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-165a97fdf6b2439496631f9924f52941 |
| Source note | uspto-grants-1987_05 |