HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,5-Trichloronitrobenzene → HCID 53714063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,5-Trichloronitrobenzene | HCID 6983 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 53714063 | HCID 53714063 | — |
Reaction Steps
0.9 mole (67.6 g) of 2-methoxyethylamine is heated to reflux in 30 ml of dioxane. 0.15 mole (34 g) of 1,2,4-trichloro-5-nitrobenzene is added portionwise. Heating under reflux is carried out for 4 hours. After cooling, dilution with iced water and neutralization with concentrated hydrochloric acid, the expected product is filtered off. Recrystallized from 96° ethanol, it melts at 106° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666453 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-63cb6cf8bfcb49ffaa2bc6b955aa06e1 |
| Source note | uspto-grants-1987_05 |