HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 13882129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 1-(4-chlorophenyl)-5-cyano-1H-pyrazole-4-carboxylate | HCID 13772949 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13882129 | HCID 13882129 | — |
Reaction Steps
The process of Example 2 was followed, starting with 3.7 g. of ethyl 1-(4-chlorophenyl)-5-cyano-4-pyrazolecarboxylate and 2 g. of sodium hydroxide in 60 ml. of denatured ethanol and 60 ml. of water to obtain 2.3 g. of the desired product, m.p. 249°-250° . The elemental analysis was as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666504 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-7c2bfa2ac2e345ae82f6f2612cb62314 |
| Source note | uspto-grants-1987_05 |