HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-ethylhydroxylamine hydrochloride → 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethyl-3-sulfamoylphenyl)cyclohex-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| Reactant | HCID 178458848 | HCID 178458848 | — |
| Product | 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethyl-3-sulfamoylphenyl)cyclohex-2-en-1-one | HCID 136020830 | — |
Reaction Steps
Reaction of ethoxyamine hydrochloride with 3-hydroxy-5-(2,4,6-trimethyl-3-sulfamoylphenyl)-2-propionylcyclohex-2-en-one following essentially the same procedure as that described in Example 1 part (iv) gave 2-[1-(ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethyl-3-sulfamoylphenyl)cyclohex-2-en-1-one (12). The compound was characterized by its proton magnetic resonance spectrum which is given in Table 5, Example 37.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666510 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-ccea4c91f5c94d3f8aef8f6e5415f940 |
| Source note | uspto-grants-1987_05 |