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HRID979014

反应详情

EQUATION

反应方程式

HRID 979014 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(COC(C(C)(C)C)C(C)(C)C)NC(=O)OCc1ccccc1
HCID20201229

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(N)COC(C(C)(C)C)C(C)(C)C
HCID13930701

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

N-Cbz-2-amino-2-methyl-1-[di-(t-butyl)methoxy]propane is dissolved in CH3OH and hydrogenated over 5% Pd/C in a Paar hydrogenation apparatus. When the reaction is complete the mixture is filtered through Celite and concentrated to yield 2-amino-2-methyl-1-[di-(t-butyl)methoxy]propane.

WORKUP

后处理

  1. filtrationis filtered through Celite
  2. concentrationconcentrated