HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13910807, compound → HCID 13910808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13910807 | HCID 13910807 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 13910808 | HCID 13910808 | 96% |
Reaction Steps
A solution of 7.0 g of 1,6-bis(4-hydroxy-3-nitrophenyl)hexane of Example 4 in ethyl acetate:methanol (3:1) and 400 mg of 5% palladium on carbon was hydrogenated on a Parr hydrogenation apparatus for 3 hours. After filtration and removal of solvent, 5.6 g of off-white solid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666909 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-b3c484c2b14c411598eb7f453a87d8ae |
| Source note | uspto-grants-1987_05 |