HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Dithionite → HCID 13842073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | HCID 178515739 | HCID 178515739 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13842073 | HCID 13842073 | — |
Reaction Steps
To a suspension of 4-hydroxy-3H-phenothiazine-3-one-5,5-dioxide (0.8 g) in a mixture of water (20 ml) and ethyl acetate (20 ml) there was added sodium dithionite (2 g) and the resulting mixture was stirred at room temperature for 20 minutes. The insoluble solid was then filtered, washed with water and dried to afford the title compound, m.p. (dec.) 261° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666907 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-35846eafa3204cf98f458366010627f6 |
| Source note | uspto-grants-1987_05 |