HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → HCID 13851365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | HCID 54295718 | HCID 54295718 | — |
| Product | HCID 13851365 | HCID 13851365 | — |
Reaction Steps
A mixture of 0.2 g (±)-[4aR*,10bS*]-1,3,4,4a,5,10b-hexahydro-9-hydroxy-2-methyl-2H-[1]benzopyrano[4,3-c]pyridine (m.p. of HCl salt 268°-269° ), 0.215 ml phenethyl alcohol and 0.3 g dicyclohexylcarboddiimide is heated under nitrogen for 18 hours at 130°. The cooled reaction mixture is flash chromatographed with CH2Cl2 /methanol (20:1) to yield the title compound; m.p. HCl salt 204°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666916 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-f0c37b45ecd64e86a01f01433f02ff68 |
| Source note | uspto-grants-1987_05 |