Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 13853698 | HCID 13853698 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13853699 | HCID 13853699 | — |
Reaction Steps
The compound of Example 1 (500 mg, 1.284 mmoles) was dissolved in a mixture of CH3OH (10 ml) and ether (10 ml) cooled to 0° C. Diazomethane was added until a slight yellow color persisted. The reaction mixture was concentrated to afford the title compound, m.p. 66°-68°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04666928 |
|---|
| Source dataset | uspto-grants-1987_05 |
|---|
| ORD ID | ord-648e7caf1fc24a1eb26ea12bbc25fc96 |
|---|
| Source note | uspto-grants-1987_05 |
|---|
