HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20191667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-(3-Chloropropyl)-6-fluorobenzo[d]isoxazole | HCID 10910880 | — |
| Reactant | 11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine | HCID 13689358 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20191667 | HCID 20191667 | — |
Reaction Steps
To 50 ml dry DMF were added 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (3.0 g, 0.0112 mole), 3-(3-chloropropyl)-6-fluoro-1,2-benzisoxazole (4.2 g, 0.02 mole), milled K2CO3 (10 g, 0.07 mole) and KI (0.01 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667039 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-cccfca7d41384d84a4e5dd96d1ae95e8 |
| Source note | uspto-grants-1987_05 |