HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20191660, compound → HCID 13689372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20191660 | HCID 20191660 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13689372 | HCID 13689372 | — |
Reaction Steps
To a cold solution of 11-[1-(4-methoxybenzoyl)piperidin-4-yl]-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (13.0 g in 100 ml THF) was added 45 ml of a 1 molar lithium aluminum hydride solution in ethyl ether. This was stirred at room temperature for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667039 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-85af7ea2cd5d4eac94c66bb6e1fc2be5 |
| Source note | uspto-grants-1987_05 |