HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13689376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoyl chloride, 3,4-dichloro- | HCID 76403 | — |
| Reactant | 11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine | HCID 13689358 | — |
| Product | HCID 13689376 | HCID 13689376 | — |
Reaction Steps
To a cold solution of 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (10.4 g; 0.04 mole in 150 ml CH2Cl2) and 6.7 ml Et3N (0.048 mole) was slowly added a solution of 3,4-dichlorobenzoyl chloride (10.05 g; 0.048 mole in 60 ml CH2Cl2). This was stirred at room temperature for 15 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667039 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-3b67ffebd0154b9d9ab58304bb8e4818 |
| Source note | uspto-grants-1987_05 |