HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 13689377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 13689376 | HCID 13689376 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 13689377 | HCID 13689377 | — |
Reaction Steps
To a cooled solution of 11-[1-(3,4-dichlorobenzoyl)piperidin-4-yl]-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (4.8 g; 0.011 mole in 100 ml THF) was added a 1 molar solution of lithium aluminum hydride in THF (17 ml, 0.017 mole). This was then stirred at room temperature for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667039 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-7eda4c7ddc834931b461852ec7e9e622 |
| Source note | uspto-grants-1987_05 |