HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 16109514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2,3-Dihydro-2,2-dimethyl-7-benzofuranol | HCID 15278 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 16109514 | HCID 16109514 | — |
Reaction Steps
To 100 ml. ethylacetate 8.23 g. (0.05 mole) 2,3-dihydro-2,2-dimethyl-7-hydroxy-benzofuran, 14.3 g. (0.1 mole) 1-bromo-2-chloro-ethane, 6.9 g. (0.05 mole) anhydrous sodium carbonate and 8.3 (0.05 mole) potassium iodide are added. The reaction mixture is heated for 30 hours and the reaction is monitored by gas chromatographic analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04668274 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-70b960008cff453986dbc65519fd4de6 |
| Source note | uspto-grants-1987_05 |