HuagongsheHuagongshe Chemistry Print Report · For research reference only
Deoxycorticosterone → Deoxycorticosterone acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Deoxycorticosterone | HCID 6166 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Product | Deoxycorticosterone acetate | HCID 5952 | 89% |
Reaction Steps
1.16 g (3.5 mmoles) of 4-pregnene-3,20-dione-21-ol [prepared as described in Step (c) above] are acetylated as described in Example 2 to give 1.16 g (89% yield) of the aimed product, m.p.: 156°-158° C., [α]D =+174° (c=1.0 in dioxane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04668437 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-f428ed2e43094318850dfe7b99c22288 |
| Source note | uspto-grants-1987_05 |