HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-2-nitrobenzaldehyde → HCID 53809505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-2-nitrobenzaldehyde | HCID 230371 | — |
| Reactant | Diethyl (3-methyl-2,5-dioxoimidazolidin-4-yl)phosphonate | HCID 13937024 | — |
| Product | HCID 53809505 | HCID 53809505 | 93% |
Reaction Steps
Reaction of 3-methoxy-6-nitrobenzaldehyde with diethyl 1-methyl-2,4-dioxoimidazolidine-5-phosphonate according to the procedure of Method D provided the title compound as a mixture of geometrical isomers, m.p. 257°-260° C. in 93% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04668686 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-0c33190502f84e6a89f3e3edd59a0050 |
| Source note | uspto-grants-1987_05 |